Pub No:
85
Title:
A Template Synthesis of Nickel 6,8,15,17-TetramethyldibenzoČ[b,i][1,4,8,11]Tetraaza-cyclotetra-2,4,7,-9,12,14-hexaene
Authors:
Cutler, A.R. and David Dolphin
Journal:
Can. J. Chem.
Year:
1977
Pages:
55, 3062-3063
Abstract:
The title Ni complex I was prepared in 31.5% yield using 2,5-dimethyl-3H-1,5-benzodiazepine, or a mixture of 1,2-(H2N)2C6H4 (II) and (MeCO)2CH2 in a template synthesis using Ni salts. The previous low yield synthesis of I required condensation of Ni bisacetylacetonate in molten II.

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